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As a leading Triethyl Phosphate TEP supplier, we deliver high-quality products across diverse grades to meet evolving needs, empowering global customers with safe, efficient, and compliant chemical solutions.
How is Triethyl Phosphate TEP prepared?
To make this product, phosphoric acid and ethanol are used as raw materials, and they are placed in a copper reactor in a ratio of 1:5. Concentrated sulfuric acid is added as a catalyst, and its amount is 3% of the total raw material. It is heated to 80 degrees to make the two react with esterification to produce water and Triethyl Phosphate TEP. The water is separated by a water separator and the reaction is continued for three hours. The process is like brewing vinegar, which requires reflux condensation to recover excess ethanol and stop the fire when no water drips out of the water separator. After the reaction, the remaining acid is neutralized, distilled and purified, and the 150-degree fraction is collected to obtain a colorless and transparent liquid with a purity of 98%. This method is like cooking soup. The taste is pure if the heat is even, so the temperature cannot be increased or decreased suddenly, otherwise impurities are easily generated.
What is the role of Triethyl Phosphate TEP in organic synthesis?
This product is a good material for ethylation reagents. In drug synthesis, it can ethylate amines, such as ethylating aniline to N-ethylaniline, with a yield of 85%. In the pesticide industry, it can ethylate phenolic compounds to synthesize insecticides, such as ethyl p-nitrophenol. Its reaction conditions are mild, no high pressure is required, it is more stable than iodoethane, and it is not easy to decompose, so it is often used in laboratories. In polymer synthesis, it is used as a polymerization initiator to regulate the molecular weight distribution of resins and make the product performance uniform. Its ethyl transfer ability is moderate and does not damage other functional groups, so it is a common product in synthetic chemistry.
What are the characteristics of Triethyl Phosphate TEP's physical properties?
This product is a colorless liquid with a slight ether fragrance, a boiling point of 150 degrees, a melting point of minus 50 degrees, good fluidity at room temperature, and no worries about crystallization. It is easily soluble in water, with a solubility of 14%. It is also easily soluble in organic solvents such as ethanol and ether, and releases heat when mixed with water. The density is about 1.07 g/cm3, which is slightly heavier than water. It is in the form of thin lines when poured and does not hang on the wall. The refractive index is 1.405, with good light transmittance. It can be used as an optical instrument cleaner to remove oil stains without damaging the lens. Its flash point is 50 degrees, and it is a flammable liquid. It needs to be stored away from fire sources, and it needs to be more careful about fire prevention than TPP.
What are the differences between the application scenarios of Triethyl Phosphate TEP and TPP?
Triethyl Phosphate TEP is mostly used in organic synthesis and solvents. Because it is easily soluble in water, it is suitable for water-based coatings and inks; Triphenyl Phosphate TPP is mostly used for plastic flame retardant. Because of its high melting point, it is suitable for resins processed at high temperatures. In the pharmaceutical field, TEP is used as an ethylating agent, and TPP is used as a drug carrier to release drug ingredients. In the textile industry, TEP can be used as a dye solvent, and TPP is used as a flame retardant finishing agent. Although both belong to the same phosphate ester, they have different application areas due to different solubility and stability, just like birds of the same genus, but one is good at singing and the other is good at flying, each suitable for its own use.
What are the specifications for the storage and transportation of Triethyl Phosphate TEP?
This product should be packed in galvanized iron barrels, sealed with rubber gaskets, and stored in a cool and ventilated warehouse at a temperature not exceeding 25 degrees, away from oxidants and fire sources. The warehouse should be equipped with fire extinguishers, and open flame operations are prohibited. It should not be transported in the same vehicle as strong acids. The barrel should be labeled "flammable liquid" and handled with care during loading and unloading to prevent impact and leakage. In case of leakage, it should be covered with sand and not flushed with water to prevent flow and spread. Its steam is irritating, so you need to wear a gas mask when operating it, such as a face mask to prevent dust, and you need to be careful.