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As a leading Trimethyl Phosphate TMP supplier, we deliver high-quality products across diverse grades to meet evolving needs, empowering global customers with safe, efficient, and compliant chemical solutions.
What details should be paid attention to when preparing Trimethyl Phosphate TMP?
This product is made by using phosphoric acid and methanol as materials, placing them in a copper reactor in a ratio of 1:4, and adding a small amount of aluminum chloride as a catalyst. The reactor is sealed and heated to 80 degrees to react to produce water and Trimethyl Phosphate TMP. Excess methanol is recovered through a condenser and the reaction is continued for three hours. The process is like evaporation, and the temperature must be strictly controlled. If it is too high, the methanol will evaporate too quickly, and if it is too low, the reaction will be incomplete. After the reaction, it is distilled and purified, and the 190-degree fraction is collected to obtain a colorless and transparent liquid with a purity of up to 99%. If the reactor leaks, the yield will be greatly reduced, so the sealing technique is essential, just like sealing the jar when brewing vinegar, and only when there is no leakage can the pure taste be obtained.
What role does Trimethyl Phosphate TMP play in organic synthesis?
This product is a good material for methylation reagents. In drug synthesis, it can convert hydroxyl groups into methoxy groups, such as methylating phenol to anisole, with a yield of 90%. In the dye industry, it can methylate amine compounds, change the color, and make azo dyes brighter. Its reaction conditions are mild, no high temperature and high pressure are required, it is safer than methyl iodide, and it is not easy to explode, so it can be used in both laboratories and industries. In polymer synthesis, it is used as a chain transfer agent to regulate the molecular weight of polymers and make the resin performance more stable. Its methyl transfer ability is moderate and does not harm other functional groups, so it is valued by synthetic chemists.
What are the characteristics of the physical properties of Trimethyl Phosphate TMP?
This product is a colorless liquid with a slight ether fragrance, a boiling point of 190 degrees, a melting point of minus 40 degrees, good fluidity at room temperature, and no worry about crystallization. It is insoluble in water, easily soluble in organic solvents such as ethanol and acetone, and miscible with ether in any proportion. Its density is about 1.21 g/cm3, slightly heavier than water, and it is linear when poured, without wall hanging phenomenon. The refractive index is 1.397, and the transmittance is high. It can be used as an optical instrument cleaning agent to remove oil stains without damaging the lens. The volatility is lower than that of TBP, so it is less likely to be lost during storage. If properly sealed, the annual loss rate does not exceed 1%.
Why is Trimethyl Phosphate TMP suitable as a flame retardant?
This product contains up to 21% phosphorus, and its flame retardant efficiency far exceeds that of general phosphorus flame retardants. When added to polyurethane foam, only 5% is needed to pass the UL94 V-0 test. When burned, it generates a phosphate protective layer to block oxygen and insulate heat. In epoxy resin, it can work synergistically with the curing agent to not only flame retardant but also enhance the cross-linking density, thereby increasing the compressive strength of the material by 10%. It has good compatibility with the resin, no precipitation after curing, and does not affect the appearance of the material. Therefore, it is often used in electronic component packaging to prevent short circuit fire and protect circuit safety.
What are the specifications for the storage and transportation of Trimethyl Phosphate TMP?
This product needs to be stored in brown glass bottles or polyethylene barrels, away from direct sunlight, and prevent decomposition by light. Store in a cool warehouse with a temperature not exceeding 30 degrees, isolated from oxidants and strong acids. Do not transport it in the same vehicle as edible chemicals. The barrel must be labeled "flammable liquid". Handle it with care during loading and unloading to prevent collision and leakage. If it is accidentally spilled, cover it with sand to absorb it. Do not flush it with water to prevent it from seeping into the ground and contaminating the water source. Its steam is slightly irritating, so you need to wear a mask when operating it. Therefore, you need to be careful when storing and transporting it, just like protecting a treasure, to prevent damage and harm.